Cinnamoyl chloride
Cinnamyl chloride is an organic compound, the molecular formula is C9H7ClO.
Derived from the reaction of with oxalyl chloride. Blend oxalyl chloride and benzene into a solution, add the dried sodium cinnamate several times with stirring from time to time, add each time until the reaction releases carbon dioxide and then add the next time. Then reflux for 2h. After a little cold, the produced sodium chloride and a small amount of unreacted sodium cinnamate were filtered off. The filtrate was first distilled off benzene under normal pressure, and then distilled under reduced pressure to collect a 131 ° C (1.47kPa) fraction, and the product was obtained with a yield of 75-90%. When purification is required, it can be recrystallized from carbon tetrachloride. Cinnamic acid is reacted with dichlorosulfoxide to prepare cinnamoyl chloride.
SPECIFICATIONSof
Cinnamoyl chloride
CAS registration number: 102-92-1
Molecular formula: C9H7ClO
Molecular weight: 166.60
Chinese name: cinnamoyl chloride; 3-phenyl-2-acryloyl chloride
English alias: 3-Phenyl-2-propenoyl chloride
EINECS registration number: 203-065-5
FEMA accession number: 2007
Melting point: 33-37 & ordm; C
Boiling point: 256-258 & ordm; C
Content: ≥98%
Properties: white or light yellow crystal.
Water-soluble: soluble in petroleum ether, carbon tetrachloride and hot ethanol, insoluble in water. Slowly decomposes in water.
APPLICATION
It can be used as an intermediate in organic synthesis, a reagent for determining trace moisture.
Tags:
Send product request
Other supplier products
 |
Cinnamamide | Cinnamamide, a non-lethal repellent, deters feeding by a wide range of avian species;cinnamamide has the potential for use against the commensa... |
 |
China Cinnamyl Acetate | Cinnamyl acetate is also known as 3-Phenyl-2-propenyl acetate; 3-Phenylallyl acetate; cinnamyl alcohol acetate; 1-Acetoxy-3-phenyl-2-propene. The... |
 |
Cinnamyl acetate | Cinnamyl acetate is also known as 3-Phenyl-2-propenyl acetate; 3-Phenylallyl acetate; cinnamyl alcohol acetate; 1-Acetoxy-3-phenyl-2-propene. T... |
 |
Phenethyl cinnamate | Product Descriptions: (C6H5CH=CHCO2CH2CH2C6H5) is a white crystal with a melting point of 215°C. Soluble in hot ethanol and oil, soluble... |
 |
2-Bromocinnamic acid | 2-Bromocinnamic-acid (C9H7BrO2) is a white crystal with a melting point of 215 °C. Insoluble in water, soluble in ethanol and hot oil. It i... |
Same products
 |
High-quality Magnesium Citrate Granules | Seller: Zhengzhou Ruipu Biological Engineering Co.,Ltd | Product Name:Magnesium Citrate Granules Description Raw material :Magnesium Citrate, Corn Starch,... |
 |
High-purity Calcium Citrate Granules | Seller: Zhengzhou Ruipu Biological Engineering Co.,Ltd | Product Name:Calcium Citrate Granules Description Raw material :calcium citrate, maltodextrin, CM... |
 |
Zinc Gluconate Granules Factory | Seller: Zhengzhou Ruipu Biological Engineering Co.,Ltd | Product Name:Zinc Gluconate Granules Description Raw material :zinc gluconate Assay:NLT 95% Shelf... |
 |
Magnesium Lactate Granules | Seller: Zhengzhou Ruipu Biological Engineering Co.,Ltd | Product Name:Magnesium Lactate Granules Description Raw material :magnesium lactate, maltodextrin... |
 |
Nisin 1414-45-5 25kg | Seller: Hebei Shengxue Dacheng Pharmaceutical Co., Ltd. | Nisin, as a natural antimicrobial peptide, finds applications in various industries due to its ab... |
